Background of the Invention
1. Field of the Invention
The present invention relates to an ultrasonic microscope having a focusing mechanism and using a cryogenic fluid as a medium for transmission of an ultrasonic beam.
2. Description of the Related Art
Japanese Patent Publication No. 59-44582 and Japanese Patent Disclosure No. 58-196453 disclose ultrasonic microscopes in which a sample is two-dimensionally scanned with an ultrasonic beam, and the waves passing through, or reflected from, the sample are processed to form an image of the sample.
In these microscopes, the ultrasonic beam must be focused onto the sample in order to form a clear image of the sample. To achieve a successful focusing of the beam, it is necessary to adjust, with high accuracy, the distance between beam-focusing means, e.g., an acoustic lens, and a surface or an internal plane of the sample, thus setting this distance within the focal depth of the microscope. The Journal of Acoustic Society of America, Vol. 67 (1980), pp. 1629-37, discloses a cryogenic ultrasonic microscope which can provide a high-resolution ultrasonic image of a sample. To conduct the ultrasonic beam from the acoustic lens to the sample efficiently, a beam-transmitting medium is filled in the gap between the acoustic lens and the sample. The beam transmitting medium is cryogenic liquid such as liquid nitrogen, liquid argon, or liquid helium, which transmits sound more slowly and absorbs less than water.
The cryogenic ultrasonic microscope also has a focusing mechanism. The mechanism is located outside the housing containing the cryogenic liquid. Due to the position of the focusing mechanism, the microscope as a whole is complex in structure, and heat can easily propagate into the housing. Hence, the temperature of the cryogenic liquid is likely to rise, making it impossible to accomplish high-accuracy focusing of the ultrasonic beam.
Summary of the Invention
Accordingly, the object of the present invention is to provide an ultrasonic microscope which has a simple structure, uses a cryogenic liquid as beam-transmitting medium, and can achieve high-accuracy focusing of an ultrasonic beam.
Brief Description of the Drawings
FIG. 1 is a sectional view illustrating an ultrasonic microscope according to the present invention; and
FIG. 2 is a sectional view showing another ultrasonic microscope according to this invention.
Detailed Description of the Preferred Embodiments
An ultrasonic microscope, which is an embodiment of the invention, will now be described with reference to FIG. 1. As is shown in this Figure, the microscope comprises a support plate 1 and a housing or adiabatic vessel 2 removably secured to the plate 1, with its opening closed by the plate 1. The vessel 2 is sealed in airtight fashion from the support plate 1, and no heat can propagate from outside into the adiabatic vessel 2. The adiabatic vessel 2 is almost completely filled with cryogenic liquid 3 such as liquid nitrogen or liquid helium, which is used as medium for transmitting an ultrasonic beam.
The adiabatic vessel 2 contains a frame unit 4 which is immersed in the cryogenic liquid 3. The frame unit 4 is formed of an upper frame 5 and a lower frame 6, both being rectangular. The unit 4 is, as a whole, rectangular, extending in vertical direction. As is evident from FIG. 1, the frame unit 4 is suspended from the support plate 1. Alternatively, the unit 4 can be mounted on, and secured to, the bottom of the adiabatic vessel 2. Further, the unit can be a hollow cylinder as a whole.
A focusing mechanism 7 (i.e., a voice-coil mechanism) is held within the upper frame 5. This mechanism 7 has two yokes 8 and 9. The upper yoke 8 and the lower yoke 9 are fastened to the upper and lower horizontal plates of the upper frame 5, respectively. The upper yoke 8 has three arms extending downward, parallel to one another. A permanent magnet 10 is embedded in the proximal portion of the center arm. The lower yoke 9 also has three arms extending upward, parallel to one another. These three arms are opposite to the three arms of the upper yoke 8. The center arm of the lower yoke 9 has a vertical guide hole 11 extending through the lower yoke 9. A hollow cylindrical permanent magnet 12 is embedded in the lower yoke 9 and located coaxial with the guide hole 11. The left and right arms of either yoke can be continuous to each other in a horizontal plane, thus forming, for example, a hollow cylinder.
A movable shaft 13 is located vertically within the frame unit 4. The shaft 13 is supported by two leaf springs 14 and 15 connected to the inner side of the frame unit 4, and can move up and down. The shaft 13 includes a hollow cylindrical upper portion, an intermediate portion, and a thin lower portion.
The center arm of the upper yoke 8 is loosely inserted in the upper portion 13a of the movable shaft 13. An upper coil 16 is wound around the upper portion 13a of the shaft 13. The coil 16 is electrically connected to a drive circuit 20 located outside the adiabatic vessel 2 and having a DC-power source. When a current is supplied from the circuit 20 to the upper coil 16, the coil 16 generates a magnetic field. This magnetic field cooperates with the magnetic field of the permanent magnet 10, to move the shaft 13 up or down against the bias of the leaf springs 14 and 15, for a distance proportional to the amount of the current flowing through the upper coil 16.
The lower portion of the movable shaft 13 extends via the vertical guide hole 11 into the lower frame 6. A sample 17 is attached to the tip of this lower end portion. A hollow cylinder 18 is coaxially secured to the intermediate portion of the movable shaft 13, and surrounds the center arm of the lower yoke 9, which in turn surrounds the lower end portion of the shaft 13. A lower coil 19 is wound around the cylinder 18. The lower coil 19 cooperates with the magnetic field of the permanent magnet 12, to generate an electrical current when the shaft 13 moves up or down. This current is proportional to he speed at which the shaft 13 moves. The lower coil 19 is connected to the input of the drive circuit 20. Therefore, the current generated by the lower coil 19 is supplied to the drive circuit 20. As a result of this, the circuit 20 controls the current supplied to the upper coil 16 in accordance with the current the coil 19 has generated, thereby to stop the movable shaft 13. In other words, the lower coil 19 locks the shaft 13 at the position to which the shaft 13 has been moved by means of the upper coil 16.
The lower frame 6 contains an acoustic lens 21 which comprises a piezoelectric transducer (not shown). The acoustic lens 21 is attached to the upper end of an X-Y scanner 22 which is secured to the lower frame 6. The X-Y scanner 22 is positioned such that the lens 21 is spaced apart from the sample 17 by a predetermined distance. The cryogenic liquid 3 fills the gap between the sample 17 and the acoustic lens 21. The acoustic lens 21 is of a known type. It applies an ultrasonic beam to the sample 17, receives the waves reflected from the sample 17 and converts these waves into electrical signals representing the intensities of the waves. The X-Y scanner 22 can move in a horizontal plane, in an x-direction and a y-direction. Hence, the acoustic lens 21 can also move in a horizontal plane, thereby to scan the sample 17 with the ultrasonic beam.
The X-Y scanner 22, which has such a structure as is shown in the mentioned Journal of Acoustic Society of America article, can serve to position the two-dimensional plane of the acoustic lens 21 parallel to the surface of the sample 17. More specifically, it moves in the x-direction and the y-direction, thus moving the lens 21 in the horizontal plane, and detects the values of the V (Z) signals generated when the lens 21 is located at several positions with respect to the sample 17. Based on observation of the V(Z) signals on an oscilloscope CRT 23, an operator can adjust the drive circuit 20 to move the focusing mechanism 7 until the V (Z) signals come to have the same value, thus indicating that the two-dimensional plane of the lens 21 is parallel to the surface of the sample 17.
The CRT (Cathode Ray Tube) 23 is connected through scanner 22 to the output of the acoustic lens 21, for displaying the wave form of the voltage output by the acoustic lens 21. This voltage is the highest when the ultrasonic beam is focused on the surface of the sample 17. Therefore, an operator turns a dial connected to a variable resistor (not shown), thus changing the current input from the drive circuit 20 to the upper coil 16, up until the waveform of the voltage display on the CRT 23 has the highest peak.
FIG. 2 illustrates a second embodiment of the present invention, which is identical to the first embodiment (FIG. 1), except for the focusing mechanism. The focusing mechanism 7 used in the second embodiment has two bobbins 30 and 31 made of non-magnetic material and connected to the upper end and middle portion of a movable shaft 13, respectively. An upper coil 16a is wound around the bobbin 30 which extends horizontally. Similarly, a lower coil 19a is wound around the bobbin 31 which extends horizontally.
Two yokes 8a and 9a are fastened to the inner surface of a rectangular frame 4 and surround the bobbins 30 and 31, respectively. A pair of permanent magnets 40a and 41a are attached to the yokes 8a, opposing the ends of the upper coil 16a. A pair of permanent magnets 40b and 41b are attached to the yoke 8a in a similar manner. The magnets 40a and 41b are positioned with their N poles facing the S poles of the magnets 41a and 40b. Hence, a magnetic flux passes through the upper coil 16a from the magnet 40a to the magnet 41a, and another magnetic flux passes through the coil 16a from the magnet 41b to the magnet 40b.
Further, a pair of permanent magnets 40a and 41a, and a pair of magnets 40b and 41b are attached to the yokes 9a and oppose the ends of the lower coil 19a. Two magnetic fluxes pass through the coil 19a in the opposite directions between the magnets 40a and 40b, on the one hand, and the magnets 41a and 41b, on the other. When an electrical current is supplied to the upper coil 16a, the coil 16a generates a magnetic field. This magnetic field and the magnetic fluxes of the magnets 40a, 40b, 41a, and 41b cause the shaft 13 to move vertically against the leaf springs 14 and 15, for the distance proportional to the amount of the current supplied to the upper coil 16a.
The lower coil 19a is used to lock the shaft 13 at the position to which the shaft 13 has been moved vertically, as in the first embodiment illustrated in FIG. 1. The X-Y scanner of the second embodiment (FIG. 2) is identical in structure with its counterpart of the first embodiment.
In either embodiment described above, the acoustic lens, the sample, the focusing mechanism, and the X-Y scanner are located within the same frame. Both the focusing mechanism and the X-Y scanner, for adjusting the positional relationship between the acoustic lens and the sample, can be remote-controlled in accordance with electrical signals externally supplied. Furthermore, the frame is entirely immersed in the cryogenic liquid. Hence, no heat can propagate into the frame to raise the temperature of the liquid. Therefore, the ultrasonic beam can be accurately focused on the sample.
The coils, used in either embodiment as means for moving the shaft supporting the sample, generate heat while electrical currents are flowing through them. In view of this, it is desirable that these coils be made of superconductive wires.